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Application 1 (+)-1-Phenyl-1-propanol / (-)-1-Phenyl-1-Propanol, various e:e
Application 2 Trans-stilbenoxide, enantiomeric separation
Application 3 Chlormezanone, enantiomeric separation
Application 4 Oxazepam, enatiomeric separation
Application 5 Androgene (various), separation
Application 6 Optical purity, UV versus rotation (alfa)
Application 7 Ketoprofene, various concentrations
Application 8 5-Methyl-5-phenylhydantoin
Application 9 unknown sample ( 2 chiral centers)
Application 10 Labetalol ( 2 Diastereometric pairs )
Application 11 Chiral Detectors (various), comparative test
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1
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CHIRALYSER (426 nm) Sample : (+)-1-Phenyl-1-propanol
(-)-1-Phenyl-1-propanol
RANGE=0128 Column : LiChrosphere , 250x4.6
AVERAGE=5 Eluent : MeOH / H2O , 80:20 , 1 ml/min

Inject : 10 µl (1g/l)



2
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CHIRALYSER Sample : Trans-stilbenoxid
RANGE=0256 Column : Chira-GROM-2, 15µm , 250x4.6
AVERAGE=6 Eluent : Heptane:2-Propanol, 95:5, 1 ml/min

Inject : 5 µl (0.5g/l)



3
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CHIRALYSER Sample : Chlormezanone
RANGE=0256 Column : Chira-GROM-3, 15µm, 250x4,6
AVERAGE=6 Eluent : EtOH:ACN, 99:1, 0.6 ml/min

Inject : 3 µl (1.6g/l)



4
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CHIRALYSER Sample : Oxazepam
RANGE=0256 Column : Chira-GROM-2, 15µm, 250x4.6
AVERAGE=6 Eluent : ACN / H2O , 50 : 50, 0.1 % TFA, 0.6ml/min

Inject : 10 µl (1.2g/l)



5
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CHIRALYSER (436 nm) Sample : Androgene (various)
RANGE=0128 Column : LiChrospere , 125x4.6
AVERAGE=5 Eluent : ACN / H2O , 70:30 , 1 ml/min

Inject : 5 µg (each compound) in 10 µl



6
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CHIRALYSER Sample : see struc. formula
RANGE=0128 Column : Cellulosetribenzoat, 250 x 8
AVERAGE=10 Eluent : MeOH, 1 ml/min
UV at 320 nm Inject : 0.44 mg in 50µl



7
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CHIRALYSER (436 nm) Sample : Ketoprofene
RANGE= various Column : Chirapak AD, 250x4.6
AVERAGE=5 Eluent : n-hexane/ethanol/TFA (80/20/0.01), 1ml/min

Inject : various concentration in 20 µl



8
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CHIRALYSER (436 nm) Sample : 5-Methly-5-phenlyhydantoin
RANGE=0128 Column : Chirobiotic T , 250x4.6
AVERAGE=5 Eluent : Methanol (100%) , 1 ml/min

Inject : 10 µg in 10 µl



9
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CHIRALYSER (436 nm) Sample : unknown (2 chiral centers)
RANGE=0128 Column : Chirobiotic T , 250x4.6
AVERAGE=5 Eluent : Methanol (100%) , 1 ml/min

Inject : 10 µg in 10 µl



10
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CHIRALYSER (436 nm) Sample : Labetalol
RANGE=0128 Column : Chirobiotic V , 250x4.6
AVERAGE=5 Eluent : MeOH / AFTA (100/0.1) , 1 ml/min

Inject : 10 µg in 10 µl



11
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Chiral Detectors / Comparative test Sample : polymere mixture
CHIRALYSER (blue) inject : 379,7 mg/l
Competitor P (green) inject : 966,9 mg/l
Competitor J (black) inject : 617,0 mg/l